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BOOK
Author Duddeck, H. (Helmut)
Title Structure elucidation by modern NMR : a workbook / H. Duddeck, W. Dietrich, G. Tóth.
Imprint Darmstadt : Steinkopff ; [New York] : Springer, [1998]
©1998
Edition Third, revised and updated edition.

LOCATION CALL # STATUS MESSAGE
 MUSKINGUM QUARTO  QD96.N8 .D813 1998    AVAILABLE  NON-CIRC
LOCATION CALL # STATUS MESSAGE
 MUSKINGUM QUARTO  QD96.N8 .D813 1998    AVAILABLE  NON-CIRC
Author Duddeck, H. (Helmut)
Subject Nuclear magnetic resonance spectroscopy -- Problems, exercises, etc.
Chemical structure -- Problems, exercises, etc.
Alt Name Dietrich, W. (Wolfgang)
Tóth, G. (Gábor), 1942-
Description 211 pages : illustrations ; 27 cm
Edition Third, revised and updated edition.
Bibliography Note Includes bibliographical references and indexes.
ISBN 379851111X
OCLC # 40168000
Table of Contents
 Foreword 
1Introduction1
2Methodology7
 2.1High Magnetic Fields8
 2.2One-Dimensional [superscript 1]H and [superscript 13]C NMR Spectra (INEPT, DEPT)10
 2.3Two-Dimensional [superscript 1]H, [superscript 1]H Correlation (COSY, Linear Prediction, Pulsed Field Gradients, TOCSY)15
 2.4Two-Dimensional [superscript 13]C, [superscript 1]H One-Bond Correlation (HETCOR, Inverse Detection, HSQC, HMQC, HMQC-TOCSY)23
 2.5Two-Dimensional [superscript 13]C, [superscript 1]H Long-Range Correlation (COLOC, HMBC)29
 2.6[superscript 13]C, [superscript 13]C-Correlation (INADEQUATE)32
 2.7Dipolar Coupling Experiments (NOE difference, NOESY, ROESY)35
 2.8Appendix: [superscript 1]H and [superscript 13]C NMR Data of Quinidine42
3Demonstration Examples44
 3.1Formation of a Novel Benzothiazoline Derivative by Ring Contraction44
 3.2Structure Elucidation of a Triterpene Saponin54
4Exercises71
5Strategies161
6Solutions167
 Explanation of Acronyms203
 Subject Index204
 Compound Index206



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