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LEADER 00000cam  2200685Ii 4500 
001    262691788 
003    OCoLC 
005    20181101045552.1 
006    m     o  d         
007    cr cn||||||||| 
008    081017s2006    gw a    ob    001 0 eng d 
010    |z2005933893 
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020    9783540262183 
020    3540262180 
020    3540234322|q(hd. bd.) 
020    9783540234326|q(hd. bd.) 
020    6610625514 
020    9786610625512 
024 3  |z9783540234326 
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037    978-3-540-23432-6|bSpringer|nhttp://www.springerlink.com 
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049    MAIN 
050  4 QP519.9.U47|bM33 2006eb 
060  4 QY 90|bM151a 2006 
072  7 QD|2lcco 
072  7 SCI|x013010|2bisacsh 
082 04 543.2|222 
100 1  Mächtle, Walter.|0http://id.loc.gov/authorities/names/
       no2006055539 
245 10 Analytical ultracentrifugation of polymers and 
       nanoparticles /|cWalter Machtle, Lars Borger. 
264  1 Berlin ;|aNew York :|bSpringer,|c2006. 
300    1 online resource (xiii, 237 pages) :|billustrations. 
336    text|btxt|2rdacontent 
337    computer|bc|2rdamedia 
338    online resource|bcr|2rdacarrier 
340    |gpolychrome|2rdacc|0http://rdaregistry.info/termList/
       RDAColourContent/1003 
347    text file|2rdaft|0http://rdaregistry.info/termList/
       fileType/1002 
490 1  Springer laboratory 
504    Includes bibliographical references and index. 
505 0  Cover -- Table of Contents -- 1 INTRODUCTION -- 1.1 
       Historic Examples of Ultracentrifugation -- 1.1.1 
       Investigations on Gold Colloids in 1924 -- 1.1.2 
       Investigations on the Structure of DNA in 1957 -- 1.2 
       Basic Theory ofUltracentrifugation -- 1.2.1 Svedberg's 
       Simplified Theory -- 1.2.2 Derivation of Lamm's Equation -
       - 1.3 Basic Experiment Types of Ultracentrifugation -- 
       1.3.1 Sedimentation Velocity Experiment -- 1.3.2 Synthetic
       Boundary Experiment -- 1.3.3 Sedimentation Equilibrium -- 
       1.3.4 Density Gradient -- 1.3.5 Approach-to-Equilibrium(or
       Archibald)Method -- 1.4 Closing Remarks -- References -- 2
       ANALYTICAL ULTRACENTRIFUGATION, INSTRUMENTATION -- 2.1 
       Ultracentrifuges -- 2.1.1 The Beckman-CoulterOptima XL-A/I
       -- 2.1.2 User-Made Centrifuges -- 2.2 Rotors -- 2.3 
       Measuring Cells -- 2.4 Detectors -- 2.4.1 AbsorptionOptics
       -- 2.4.2 Interference Optics -- 2.4.3 Schlieren Optics -- 
       2.4.4 OtherDetectors -- 2.5 Multiplexer -- 2.6 
       AuxiliaryMeasurements -- 2.6.1 Measurement of the Solvent 
       Density and the Partial Specific Volume -- 2.6.2 
       Measurement of the Refractive Index and the Specific 
       Refractive Index Increment -- References -- 3 
       SEDIMENTATION VELOCITY -- 3.1 Introduction -- 3.2 Basic 
       Example of Sedimentation Velocity -- 3.2.1 Determination 
       of s -- 3.2.2 Standard Conditions for s Estimation -- 
       3.2.3 Radial Dilution and Thickening -- 3.2.4 
       Concentration Dependence -- 3.3 Advanced Theory of 
       Sedimentation Velocity Runs -- 3.3.1 Johnston-Ogston 
       Effect -- 3.3.2 Self-Sharpening of Boundaries -- 3.3.3 
       Pressure Dependence -- 3.3.4 Speed Dependence -- 3.3.5 
       Charge Effects -- 3.3.6 Separation of Sedimentation and 
       Diffusion -- 3.3.7 Test of Homogeneity -- 3.4 
       Sedimentation Velocity Runs of Macromolecules to Measure 
       Average M and MMD -- 3.4.1 Evaluation of the Average Molar
       Mass M by Sedimentation Velocity Runs via Scaling Laws -- 
       3.4.2 Evaluation of Molar Mass Distributions (MMD) by 
       Sedimentation Velocity Runs via Scaling Laws -- 3.5 
       Sedimentation Velocity Runs on Particles to Measure 
       Average d[sub(p)] and PSD -- 3.5.1 Particle Size 
       Distribution via AUC Turbidity Detector and Mie Theory -- 
       3.5.2 Coupling Technique to Measure very Broad PSD -- 
       3.5.3 H[sub(2)]O-D[sub(2)]O Density Variation Method to 
       Measure Particle Densities via Sedimentation Velocity Runs
       -- 3.5.4 PSD Measurement of very Small Platinum Clusters 
       Using UVOptics -- 3.6 Synthetic Boundary Experiments -- 
       3.6.1 Synthetic Boundary Crystallization 
       Ultracentrifugation -- References -- 4 DENSITY GRADIENTS -
       - 4.1 Introduction -- 4.2 Static Density Gradients -- 
       4.2.1 Theory of StaticDensity Gradients -- 4.2.2 Gradient 
       Materials -- 4.2.3 Experimental Procedure -- 4.2.4 
       Examples -- 4.3 Dynamic Density Gradients -- 4.4 Other 
       Types of Den. 
520 8  Annotation|bAnalytical ultracentifugation (AUe is a 
       powerful method for the characterization of polymers, 
       biopolymers, polyelectrolytes, nanoparticles, dispersions,
       and other colloidal systems. The method is able to 
       determine the molar mass, the particle size, the particle 
       density and interaction parameters like virial 
       coefficients and association constants. Because AUC is 
       also a fractionation method, the determination of the 
       molar mass distribution, the particle size distribution, 
       and the particle density distribution is possible. A 
       special technique, the density gradient method, allows 
       fractionating heterogeneous samples according to their 
       chemical nature that means being able to detect chemical 
       heterogeneity. The book is divided into chapters 
       concerning instrumentation, sedimentation velocity runs, 
       density gradient runs, application examples and future 
       developments. In particular, the detailed application 
       chapter demonstrates the versatility and power of AUC by 
       means of many interesting and important industrial 
       examples. Thus the book concentrates on practical aspects 
       rather than details of centrifugation theory. Both authors
       have many years of experience in an industrial AUC 
       research laboratory of a world leading chemical company. 
588 0  Print version record. 
650  0 Ultracentrifugation.|0http://id.loc.gov/authorities/
       subjects/sh89000198 
650  0 Polymers|xAnalysis.|0http://id.loc.gov/authorities/
       subjects/sh2008109762 
650  0 Nanoparticles|0http://id.loc.gov/authorities/subjects/
       sh85089689|xAnalysis.|0http://id.loc.gov/authorities/
       subjects/sh2002006221 
650 12 Ultracentrifugation|xmethods.|0https://id.nlm.nih.gov/mesh
       /D014461Q000379 
650 22 Polymers|xanalysis.|0https://id.nlm.nih.gov/mesh/
       D011108Q000032 
650 22 Nanostructures|xanalysis.|0https://id.nlm.nih.gov/mesh/
       D049329Q000032 
655  4 Electronic books. 
655  7 Textbooks.|2fast|0http://id.worldcat.org/fast/1423863 
700 1  Börger, L.|0http://id.loc.gov/authorities/names/
       nb2004310502 
773 0  |tSpringer e-books 
776 08 |iPrint version:|aMachtle, Walter.|tAnalytical 
       ultracentrifugation of polymers and nanoparticles.|dBerlin
       ; New York : Springer, 2006|z3540234322|z9783540234326
       |w(DLC)  2005933893|w(OCoLC)64571899 
830  0 Springer laboratory.|0http://id.loc.gov/authorities/names/
       n92078049 
990    SpringerLink|bSpringer English/International eBooks 2006 -
       Full Set|c2018-10-31|yNew collection 
       springerlink.ebooks2006|5OH1 
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