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LEADER 00000cam 2200685Ii 4500
001 262691788
003 OCoLC
005 20181101045552.1
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007 cr cn|||||||||
008 081017s2006 gw a ob 001 0 eng d
010 |z2005933893
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020 9783540262183
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020 9783540234326|q(hd. bd.)
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037 978-3-540-23432-6|bSpringer|nhttp://www.springerlink.com
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049 MAIN
050 4 QP519.9.U47|bM33 2006eb
060 4 QY 90|bM151a 2006
072 7 QD|2lcco
072 7 SCI|x013010|2bisacsh
082 04 543.2|222
100 1 Mächtle, Walter.|0http://id.loc.gov/authorities/names/
no2006055539
245 10 Analytical ultracentrifugation of polymers and
nanoparticles /|cWalter Machtle, Lars Borger.
264 1 Berlin ;|aNew York :|bSpringer,|c2006.
300 1 online resource (xiii, 237 pages) :|billustrations.
336 text|btxt|2rdacontent
337 computer|bc|2rdamedia
338 online resource|bcr|2rdacarrier
340 |gpolychrome|2rdacc|0http://rdaregistry.info/termList/
RDAColourContent/1003
347 text file|2rdaft|0http://rdaregistry.info/termList/
fileType/1002
490 1 Springer laboratory
504 Includes bibliographical references and index.
505 0 Cover -- Table of Contents -- 1 INTRODUCTION -- 1.1
Historic Examples of Ultracentrifugation -- 1.1.1
Investigations on Gold Colloids in 1924 -- 1.1.2
Investigations on the Structure of DNA in 1957 -- 1.2
Basic Theory ofUltracentrifugation -- 1.2.1 Svedberg's
Simplified Theory -- 1.2.2 Derivation of Lamm's Equation -
- 1.3 Basic Experiment Types of Ultracentrifugation --
1.3.1 Sedimentation Velocity Experiment -- 1.3.2 Synthetic
Boundary Experiment -- 1.3.3 Sedimentation Equilibrium --
1.3.4 Density Gradient -- 1.3.5 Approach-to-Equilibrium(or
Archibald)Method -- 1.4 Closing Remarks -- References -- 2
ANALYTICAL ULTRACENTRIFUGATION, INSTRUMENTATION -- 2.1
Ultracentrifuges -- 2.1.1 The Beckman-CoulterOptima XL-A/I
-- 2.1.2 User-Made Centrifuges -- 2.2 Rotors -- 2.3
Measuring Cells -- 2.4 Detectors -- 2.4.1 AbsorptionOptics
-- 2.4.2 Interference Optics -- 2.4.3 Schlieren Optics --
2.4.4 OtherDetectors -- 2.5 Multiplexer -- 2.6
AuxiliaryMeasurements -- 2.6.1 Measurement of the Solvent
Density and the Partial Specific Volume -- 2.6.2
Measurement of the Refractive Index and the Specific
Refractive Index Increment -- References -- 3
SEDIMENTATION VELOCITY -- 3.1 Introduction -- 3.2 Basic
Example of Sedimentation Velocity -- 3.2.1 Determination
of s -- 3.2.2 Standard Conditions for s Estimation --
3.2.3 Radial Dilution and Thickening -- 3.2.4
Concentration Dependence -- 3.3 Advanced Theory of
Sedimentation Velocity Runs -- 3.3.1 Johnston-Ogston
Effect -- 3.3.2 Self-Sharpening of Boundaries -- 3.3.3
Pressure Dependence -- 3.3.4 Speed Dependence -- 3.3.5
Charge Effects -- 3.3.6 Separation of Sedimentation and
Diffusion -- 3.3.7 Test of Homogeneity -- 3.4
Sedimentation Velocity Runs of Macromolecules to Measure
Average M and MMD -- 3.4.1 Evaluation of the Average Molar
Mass M by Sedimentation Velocity Runs via Scaling Laws --
3.4.2 Evaluation of Molar Mass Distributions (MMD) by
Sedimentation Velocity Runs via Scaling Laws -- 3.5
Sedimentation Velocity Runs on Particles to Measure
Average d[sub(p)] and PSD -- 3.5.1 Particle Size
Distribution via AUC Turbidity Detector and Mie Theory --
3.5.2 Coupling Technique to Measure very Broad PSD --
3.5.3 H[sub(2)]O-D[sub(2)]O Density Variation Method to
Measure Particle Densities via Sedimentation Velocity Runs
-- 3.5.4 PSD Measurement of very Small Platinum Clusters
Using UVOptics -- 3.6 Synthetic Boundary Experiments --
3.6.1 Synthetic Boundary Crystallization
Ultracentrifugation -- References -- 4 DENSITY GRADIENTS -
- 4.1 Introduction -- 4.2 Static Density Gradients --
4.2.1 Theory of StaticDensity Gradients -- 4.2.2 Gradient
Materials -- 4.2.3 Experimental Procedure -- 4.2.4
Examples -- 4.3 Dynamic Density Gradients -- 4.4 Other
Types of Den.
520 8 Annotation|bAnalytical ultracentifugation (AUe is a
powerful method for the characterization of polymers,
biopolymers, polyelectrolytes, nanoparticles, dispersions,
and other colloidal systems. The method is able to
determine the molar mass, the particle size, the particle
density and interaction parameters like virial
coefficients and association constants. Because AUC is
also a fractionation method, the determination of the
molar mass distribution, the particle size distribution,
and the particle density distribution is possible. A
special technique, the density gradient method, allows
fractionating heterogeneous samples according to their
chemical nature that means being able to detect chemical
heterogeneity. The book is divided into chapters
concerning instrumentation, sedimentation velocity runs,
density gradient runs, application examples and future
developments. In particular, the detailed application
chapter demonstrates the versatility and power of AUC by
means of many interesting and important industrial
examples. Thus the book concentrates on practical aspects
rather than details of centrifugation theory. Both authors
have many years of experience in an industrial AUC
research laboratory of a world leading chemical company.
588 0 Print version record.
650 0 Ultracentrifugation.|0http://id.loc.gov/authorities/
subjects/sh89000198
650 0 Polymers|xAnalysis.|0http://id.loc.gov/authorities/
subjects/sh2008109762
650 0 Nanoparticles|0http://id.loc.gov/authorities/subjects/
sh85089689|xAnalysis.|0http://id.loc.gov/authorities/
subjects/sh2002006221
650 12 Ultracentrifugation|xmethods.|0https://id.nlm.nih.gov/mesh
/D014461Q000379
650 22 Polymers|xanalysis.|0https://id.nlm.nih.gov/mesh/
D011108Q000032
650 22 Nanostructures|xanalysis.|0https://id.nlm.nih.gov/mesh/
D049329Q000032
655 4 Electronic books.
655 7 Textbooks.|2fast|0http://id.worldcat.org/fast/1423863
700 1 Börger, L.|0http://id.loc.gov/authorities/names/
nb2004310502
773 0 |tSpringer e-books
776 08 |iPrint version:|aMachtle, Walter.|tAnalytical
ultracentrifugation of polymers and nanoparticles.|dBerlin
; New York : Springer, 2006|z3540234322|z9783540234326
|w(DLC) 2005933893|w(OCoLC)64571899
830 0 Springer laboratory.|0http://id.loc.gov/authorities/names/
n92078049
990 SpringerLink|bSpringer English/International eBooks 2006 -
Full Set|c2018-10-31|yNew collection
springerlink.ebooks2006|5OH1
| ||||||||||||
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